3GRS

REFINED STRUCTURE OF GLUTATHIONE REDUCTASE AT 1.54 ANGSTROMS RESOLUTION

Replaces:  2GRSReplaces:  1GRS

Experimental procedure

Spacegroup name	B 1 1 2
Unit cell lengths	119.800, 84.500, 63.200
Unit cell angles	90.00, 90.00, 58.70

Refinement procedure

Resolution	10.000 - 1.540
R-factor	0.186 *
Rwork	0.186
RMSD bond length	0.025 *
RMSD bond angle	2.400 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.540 *
Number of reflections	78959 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	1.2 (M)
2	1	reservoir	potassium phosphate	0.1 (M)