3GA1
Crystal Structure of the Human Nac1 POZ Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9763 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 57.690, 57.690, 172.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.960 - 2.100 |
R-factor | 0.208 |
Rwork | 0.206 |
R-free | 0.24100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2if5 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.294 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (CCP4_3.3.9 2008/10/21) |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0066) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.960 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.103 | 0.506 |
Total number of observations | 17832 | |
Number of reflections | 17928 | |
<I/σ(I)> | 13.5 | 4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.7 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 291 | 6M ammonium nitrate, 0.1M bis-tris propane, pH7.5, VAPOR DIFFUSION, SITTING DROP, temperature 291K |