3G5B
The structure of UNC5b cytoplasmic domain
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-06-01 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.243, 62.710, 118.110 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.780 - 2.000 |
R-factor | 0.196 |
Rwork | 0.193 |
R-free | 0.25000 |
Structure solution method | SIRAS |
RMSD bond length | 0.009 |
RMSD bond angle | 1.185 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.074 | 0.381 |
Number of reflections | 25672 | |
Completeness [%] | 98.8 | 95.8 |
Redundancy | 6.5 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 289 | 0.4~0.5M Ammonium Phosphate, 0.1M MES Buffer, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K |