3FRY
Crystal structure of the CopA C-terminal metal binding domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 23-ID-D |
| Synchrotron site | APS |
| Beamline | 23-ID-D |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2007-10-12 |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | P 1 2 1 |
| Unit cell lengths | 40.131, 35.989, 51.262 |
| Unit cell angles | 90.00, 104.89, 90.00 |
Refinement procedure
| Resolution | 27.320 - 2.000 |
| R-factor | 0.222 |
| Rwork | 0.222 |
| R-free | 0.23800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1osd |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 9568 |
| Completeness [%] | 97.3 |
| Redundancy | 6.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.5 | 298 | 0.1M citrate, 30% PEG-6000, pH 4.5, VAPOR DIFFUSION, SITTING DROP, temperature 298.0K |
