3FR9

Tetramerization and Cooperativity in Plasmodium falciparum glutathione transferase are mediated by the atypic loop 113-118

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE X13
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	X13
Temperature [K]	100
Detector technology	CCD
Collection date	2007-08-22
Detector	MAR CCD 165 mm
Spacegroup name	P 21 21 21
Unit cell lengths	57.402, 68.352, 122.667
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.400
R-factor	0.24266
Rwork	0.240
R-free	0.29579
Structure solution method	SAD
RMSD bond length	0.006
RMSD bond angle	0.885
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.400
Number of reflections	18320

Crystallization Conditions

crystal ID	method	pH	temperature	details
1