3FQ7

Gabaculine complex of GSAM

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Wavelength(s)	0.98994
Spacegroup name	P 21 21 21
Unit cell lengths	66.372, 107.025, 121.752
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.410 - 2.150
R-factor	0.214
Rwork	0.214
R-free	0.24000
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.300
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	AMoRE
Refinement software	CNS (1.2)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.500
High resolution limit [Å]	2.150
Number of reflections	41273

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	2.8	273	pH 2.8, VAPOR DIFFUSION, temperature 273K