3FKR

Structure of L-2-keto-3-deoxyarabonate dehydratase complex with pyruvate

Experimental procedure

Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL38B1
Synchrotron site	SPring-8
Beamline	BL38B1
Temperature [K]	100
Detector technology	CCD
Detector	RIGAKU JUPITER 210
Wavelength(s)	1.0
Spacegroup name	P 31 2 1
Unit cell lengths	79.259, 79.259, 206.527
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	14.997 - 1.801
R-factor	0.1977
Rwork	0.196
R-free	0.23700
RMSD bond length	0.025
RMSD bond angle	2.047
Data reduction software	HKL-2000
Data scaling software	PROCESS
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.860
High resolution limit [Å]	1.800	1.800
Number of reflections	70047
Completeness [%]	99.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1