3FIM
Crystal structure of aryl-alcohol-oxidase from Pleurotus eryingii
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM16 |
Synchrotron site | ESRF |
Beamline | BM16 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2003-10-23 |
Detector | MARRESEARCH |
Wavelength(s) | 0.85 |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 180.226, 180.226, 160.407 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.040 - 2.550 |
R-factor | 0.17507 |
Rwork | 0.173 |
R-free | 0.20640 |
Structure solution method | SAD |
RMSD bond length | 0.035 |
RMSD bond angle | 2.693 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXS |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.700 | 37.700 |
High resolution limit [Å] | 2.390 | 2.390 |
Rmerge | 0.102 | 0.464 |
Number of reflections | 56141 | |
<I/σ(I)> | 4 | |
Completeness [%] | 97.7 | 88.8 |
Redundancy | 15 | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 295 | 1M lithium sulfate, 0.1M Bis-Tris propane, pH7.4, VAPOR DIFFUSION, SITTING DROP, temperature 295K |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 295 | 1M lithium sulfate, 0.1M Bis-Tris propane, pH7.4, VAPOR DIFFUSION, SITTING DROP, temperature 295K |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 295 | 1M lithium sulfate, 0.1M Bis-Tris propane, pH7.4, VAPOR DIFFUSION, SITTING DROP, temperature 295K |