3FCW
Crystal structure of the Mimivirus NDK N62L mutant complexed with UDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 105 |
Detector technology | CCD |
Collection date | 2007-09-10 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.934 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 80.994, 152.812, 186.554 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.073 - 2.400 |
R-factor | 0.202 |
Rwork | 0.200 |
R-free | 0.24800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b8p |
RMSD bond length | 0.006 |
RMSD bond angle | 1.129 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 76.500 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 45260 | |
<I/σ(I)> | 8.2 | 2.1 |
Completeness [%] | 99.4 | 100 |
Redundancy | 7 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 40 to 44% MPD, 0.1M Hepes, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |