3FAU
Crystal Structure of human small-MutS related domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 4A |
| Synchrotron site | PAL/PLS |
| Beamline | 4A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-05-24 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 34.490, 57.106, 71.356 |
| Unit cell angles | 90.00, 97.91, 90.00 |
Refinement procedure
| Resolution | 44.419 - 1.900 |
| R-factor | 0.19 |
| Rwork | 0.187 |
| R-free | 0.24200 |
| Starting model (for MR) | 2d9i |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.131 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.550 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.041 | 0.217 |
| Number of reflections | 42988 | |
| <I/σ(I)> | 46.607 | |
| Completeness [%] | 97.3 | 87 |
| Redundancy | 5 | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | hanging drop | 7 | 293 | 0.1M Ammonium Chloride, 0.1M Mops (pH 7.0), 40% PEG 2000mme, hanging drop, temperature 293K |
