3EVU
Crystal structure of Calcium bound dimeric GCAMP2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Detector technology | CCD |
| Collection date | 2007-06-30 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 127.936, 47.310, 69.642 |
| Unit cell angles | 90.00, 100.70, 90.00 |
Refinement procedure
| Resolution | 42.525 - 1.750 |
| R-factor | 0.164 |
| Rwork | 0.161 |
| R-free | 0.19700 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.144 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 1.810 |
| High resolution limit [Å] | 1.750 | 3.770 | 1.750 |
| Rmerge | 0.040 | 0.029 | 0.239 |
| Number of reflections | 41444 | ||
| <I/σ(I)> | 35.489 | ||
| Completeness [%] | 100.0 | 99.7 | 99.9 |
| Redundancy | 4.6 | 4.5 | 4.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
