3EUX
Crystal Structure of Crosslinked Ribonuclease A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 100.678, 32.692, 72.588 |
Unit cell angles | 90.00, 91.00, 90.00 |
Refinement procedure
Resolution | 41.700 - 1.650 |
Rwork | 0.213 |
R-free | 0.24900 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.215 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.710 |
High resolution limit [Å] | 1.650 | 3.550 | 1.650 |
Rmerge | 0.102 | 0.067 | 0.595 |
Number of reflections | 23665 | ||
Completeness [%] | 81.7 | 99.4 | 33.8 |
Redundancy | 2.6 | 3.4 | 1.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 291 | PEG 4000, sodium citrate, pH 5.0, vapor diffusion, hanging drop, temperature 291K |