Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL7-1 |
| Synchrotron site | SSRL |
| Beamline | BL7-1 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1999-10-26 |
| Detector | MAR scanner 345 mm plate |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 41.234, 41.234, 95.377 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.830 - 1.870 |
| R-factor | 0.22 |
| Rwork | 0.216 |
| R-free | 0.28200 |
| Structure solution method | MIRAS |
| RMSD bond length | 0.016 |
| RMSD bond angle | 2.142 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SHARP |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.830 | 1.940 |
| High resolution limit [Å] | 1.870 | 1.870 |
| Number of reflections | 8064 | |
| <I/σ(I)> | 13.6 | |
| Completeness [%] | 97.6 | 96.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | 298 | PEG1000, ammonium sulfate, imidazole, pH 7.0, VAPOR DIFFUSION, temperature 298K |
