3EHG
Crystal structure of the ATP-binding domain of DesK in complex with ATP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2008-02-19 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.379, 49.078, 81.436 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.030 - 1.740 |
R-factor | 0.167 |
Rwork | 0.164 |
R-free | 0.21500 |
Structure solution method | SAD |
RMSD bond length | 0.022 |
RMSD bond angle | 1.946 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.2.25) |
Phasing software | SHARP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.035 | 22.530 | 1.820 |
High resolution limit [Å] | 1.737 | 5.460 | 1.737 |
Rmerge | 0.078 | 0.032 | 0.504 |
Total number of observations | 2662 | 9812 | |
Number of reflections | 17082 | ||
<I/σ(I)> | 8.616 | 19.3 | 1.4 |
Completeness [%] | 97.0 | 96 | 84.5 |
Redundancy | 4.8 | 4.4 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 293 | pH 9, vapor diffusion, hanging drop, temperature 293K |