3EBQ
Crystal structure of human PPPDE1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-08-10 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54178 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 41.625, 41.625, 184.239 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.040 - 1.900 |
R-factor | 0.22585 |
Rwork | 0.224 |
R-free | 0.27273 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.630 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 13493 | |
<I/σ(I)> | 45.21 | 2.57 |
Completeness [%] | 98.4 | 87.9 |
Redundancy | 11.4 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | 10% PEG 4000, 0.1 M SODIUM, ACETATE, 0.1 M TRIS HCL PH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K. CRYSTALS WERE SOAKED OVERNIGHT IN 0.01 M THIMEROSAL TO CREATE THE MERCURY DERIVATIVE. |