3EB9
Crystal structure of 6-phosphogluconolactonase from trypanosoma brucei complexed with citrate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-3 |
| Synchrotron site | ESRF |
| Beamline | ID14-3 |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2006-10-01 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.931 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.460, 87.210, 64.790 |
| Unit cell angles | 90.00, 96.53, 90.00 |
Refinement procedure
| Resolution | 24.580 - 2.000 |
| R-factor | 0.1977 |
| Rwork | 0.195 |
| R-free | 0.24360 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2j0e |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.290 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | BUSTER-TNT (2.1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 24.580 | 2.052 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 36055 | |
| Completeness [%] | 100.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
