3E5W
Crystal Structure Analysis of FP611
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2008-05-27 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.96 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 71.250, 104.460, 133.320 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 62.800 - 1.710 |
| R-factor | 0.184 |
| Rwork | 0.183 |
| R-free | 0.20900 |
| Starting model (for MR) | 1uis |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.916 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | TNT |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 62.800 | 1.780 |
| High resolution limit [Å] | 1.710 | 1.710 |
| Rmerge | 0.075 | 0.748 |
| Number of reflections | 106080 | 11797 |
| <I/σ(I)> | 17.8 | 2.9 |
| Completeness [%] | 98.2 | 97.4 |
| Redundancy | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | PEG 8000, pH 4.6, vapor diffusion, hanging drop, temperature 298K |
