3E5Q
Unbound Oxidised CprK
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-06-09 |
| Detector | ADSC QUANTUM 4 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 79.405, 64.710, 148.355 |
| Unit cell angles | 90.00, 105.29, 90.00 |
Refinement procedure
| Resolution | 142.860 - 3.200 |
| R-factor | 0.26086 |
| Rwork | 0.258 |
| R-free | 0.31760 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.022 |
| RMSD bond angle | 2.302 |
| Refinement software | REFMAC (5.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 142.860 |
| High resolution limit [Å] | 3.200 |
| Number of reflections | 18436 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 100mM calcium chloride, 100mM Hepes, PEG 2000 MME, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
