3E4U
Crystal Structure of the Wild-Type Human BCL6 BTB/POZ Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-07-05 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.972 |
Spacegroup name | P 32 |
Unit cell lengths | 59.209, 59.209, 158.971 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 36.860 - 2.100 |
R-factor | 0.221 |
Rwork | 0.219 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.294 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.2.25) |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.860 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.068 | 0.157 |
Total number of observations | 20521 | |
Number of reflections | 36195 | |
<I/σ(I)> | 4.6 | |
Completeness [%] | 99.4 | 100 |
Redundancy | 3.8 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 291 | 2.5 M sodium nitrate, 100 mM sodium acetate (pH 4.5), 40 mM spermidine, VAPOR DIFFUSION, SITTING DROP, temperature 291K |