3DF6
The thermo- and acido-stable ORF-99 from the archaeal virus AFV1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-01 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.112, 97.688, 103.679 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.050 |
R-factor | 0.1915 |
Rwork | 0.191 |
R-free | 0.22106 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.440 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXS |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 2.160 |
High resolution limit [Å] | 2.050 | 2.050 |
Rmerge | 0.095 | 0.399 |
Number of reflections | 37209 | |
<I/σ(I)> | 25 | 7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.8 | 14.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.8 | 293 | 33% MPD, 0.2M CaCl2, 0.1M Hepes, pH 6.8, VAPOR DIFFUSION, SITTING DROP, temperature 293K |