3CZ6

Crystal Structure of the Rap1 C-terminus

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-D
Synchrotron site	APS
Beamline	23-ID-D
Collection date	2005-12-02
Wavelength(s)	0.9818
Spacegroup name	P 1 21 1
Unit cell lengths	48.010, 47.980, 72.560
Unit cell angles	90.00, 94.23, 90.00

Refinement procedure

Resolution	50.000 - 1.850
Rwork	0.175
R-free	0.19900
Structure solution method	SAD
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	REFMAC

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.850
Number of reflections	28230

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP			VAPOR DIFFUSION, HANGING DROP