3CLN

STRUCTURE OF CALMODULIN REFINED AT 2.2 ANGSTROMS RESOLUTION

Replaces:  1CLN

Experimental procedure

Spacegroup name	P 1
Unit cell lengths	29.710, 53.790, 24.990
Unit cell angles	94.13, 97.57, 89.46

Refinement procedure

Resolution	5.000 * - 2.200
R-factor	0.175
RMSD bond length	0.016
RMSD bond angle	0.034
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	5.000 *
High resolution limit [Å]	2.200 *
Total number of observations	7335 *
Number of reflections	6685 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	calmodulin	10 (mg/ml)
2	1	1		0.004 (M)
3	1	1	MPD	45-60 (%(v/v))
4	1	1	cacodylate	0.05 (M)
5	1	2	MPD	45-60 (%(v/v))
6	1	2	cacodylate	0.05 (M)