3BY2

Norwalk P polypeptide (228-523)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.5418
Spacegroup name	I 21 21 21
Unit cell lengths	82.799, 83.771, 102.229
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.600
Rwork	0.212
R-free	0.27080
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1ihm
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.600
Number of reflections	8083
Redundancy	1.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1