3BP9
Structure of B-tropic MLV capsid N-terminal domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 1 |
| Unit cell lengths | 86.264, 86.832, 152.360 |
| Unit cell angles | 89.12, 90.04, 60.26 |
Refinement procedure
| Resolution | 17.160 - 2.600 |
| R-factor | 0.226 |
| Rwork | 0.222 |
| R-free | 0.29200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1u7k |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.431 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.600 |
| Number of reflections | 114996 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 291 | 13-16% PEG 3350, 100mM sodium citrate pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 291K |
