3BOP
Structure of mouse beta-neurexin 2D4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4C |
Synchrotron site | NSLS |
Beamline | X4C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-10 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.9793 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 95.485, 96.983, 62.584 |
Unit cell angles | 90.00, 105.98, 90.00 |
Refinement procedure
Resolution | 20.000 - 3.000 |
R-factor | 0.215 |
Rwork | 0.211 |
R-free | 0.28900 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.029 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.116 | 0.430 |
Number of reflections | 10939 | |
<I/σ(I)> | 6.5 | 2 |
Completeness [%] | 98.7 | 99.6 |
Redundancy | 3.3 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | 15% PEG 4000, 0.2M (NH4)2SO4, 0.1M sodium acetate, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |