3BCY
Crystal structure of YER067W
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F2 |
| Synchrotron site | CHESS |
| Beamline | F2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-11-03 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9642, 0.9790, 0.9794 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 41.194, 41.194, 184.403 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.540 - 1.700 |
| R-factor | 0.198 |
| Rwork | 0.196 |
| R-free | 0.23800 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.368 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELXS |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.680 |
| High resolution limit [Å] | 1.610 | 1.610 |
| Rmerge | 0.040 | 0.109 |
| Number of reflections | 20312 | |
| <I/σ(I)> | 73.4 | 11.5 |
| Completeness [%] | 92.4 | 58.6 |
| Redundancy | 12 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 13% PEG6000, 0.2M ammonium chloride, 0.1M sodium acetate, 20% glycerol, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
