3BC1
Crystal Structure of the complex Rab27a-Slp2a
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-10-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 53.505, 77.777, 115.011 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.800 |
R-factor | 0.20145 |
Rwork | 0.199 |
R-free | 0.24474 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2if0 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.054 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.345 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.093 | 0.634 |
Number of reflections | 45347 | |
<I/σ(I)> | 6.5 | 1.25 |
Completeness [%] | 95.7 | 98.6 |
Redundancy | 2.6 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 289 | Na Citrate, Cacodylate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K |