3ATS
Crystal structure of Rv3168
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 6C1 |
Synchrotron site | PAL/PLS |
Beamline | 6C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.23985 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.738, 62.366, 103.614 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.610 - 1.670 |
R-factor | 0.19265 |
Rwork | 0.190 |
R-free | 0.23328 |
Structure solution method | SAD |
RMSD bond length | 0.023 |
RMSD bond angle | 1.747 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.730 |
High resolution limit [Å] | 1.670 | 1.670 |
Number of reflections | 46207 | |
Completeness [%] | 98.3 | 90.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 295 | PEG 3000, Ca(OAc)2, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 295 | PEG 3000, Ca(OAc)2, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K |