3AQQ
Crystal structure of human CRHSP-24
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-07-31 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97945 |
Spacegroup name | P 61 |
Unit cell lengths | 79.856, 79.856, 181.982 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.603 - 2.798 |
R-factor | 0.2307 |
Rwork | 0.229 |
R-free | 0.27240 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.266 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.798 | 2.800 |
Number of reflections | 16210 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.9 | 293 | 0.1M sodium acetate trihydrate, 2.0M sodium formate, pH 4.9, VAPOR DIFFUSION, HANGING DROP, temperature 293K |