Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2007-02-26 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.5418 |
| Spacegroup name | I 41 2 2 |
| Unit cell lengths | 133.351, 133.351, 217.759 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.800 - 2.700 |
| R-factor | 0.21553 |
| Rwork | 0.209 |
| R-free | 0.27551 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2Z9E |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.845 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.800 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmerge | 0.061 | 0.432 |
| Number of reflections | 27157 | |
| <I/σ(I)> | 20.9 | 2.4 |
| Completeness [%] | 99.8 | 99.2 |
| Redundancy | 8.7 | 4.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 5.4 | 293 | 0.2M LI2SO4, 0.1M PHOSPHATE-CITRATE pH 5.4, 10% (V/V) ISO-PROPANOL, EVAPORATION, temperature 293K |
