3ABM
Bovine heart cytochrome c oxidase at the fully oxidized state (200-s X-ray exposure dataset)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Collection date | 2003-05-19 |
Wavelength(s) | 0.9 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 183.697, 206.991, 178.251 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 1.950 |
Rwork | 0.181 |
R-free | 0.21400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2dyr |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 200.000 |
High resolution limit [Å] | 1.950 |
Number of reflections | 473853 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |