3A45
Crystal structure of MvNei1_2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-05-09 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 38.673, 54.417, 87.308 |
Unit cell angles | 107.00, 99.86, 93.42 |
Refinement procedure
Resolution | 15.000 - 2.300 |
Rwork | 0.203 |
R-free | 0.26500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a42 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.223 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.043 | 0.146 |
Number of reflections | 27932 | |
<I/σ(I)> | 17.1 | 8.1 |
Completeness [%] | 94.4 | 93.2 |
Redundancy | 2 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 285 | PEG 4000, ammonium sulfate, pH6.0, VAPOR DIFFUSION, HANGING DROP, temperature 285K |