3A1U
Crystal structue of the cytosolic domain of T. maritima FeoB iron iransporter in GMPPNP form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Collection date | 2008-02-14 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.613, 109.396, 57.261 |
| Unit cell angles | 90.00, 97.99, 90.00 |
Refinement procedure
| Resolution | 39.368 - 1.800 |
| R-factor | 0.1852 |
| Rwork | 0.183 |
| R-free | 0.21870 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3a1s |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.975 |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 48359 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 60-66% MPD, 0.1M HEPES, pH7.5, 4% 1-3-butanediol |
