3A1T
Crystal structue of the cytosolic domain of T. maritima FeoB iron iransporter in GDP form II
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Collection date | 2008-02-28 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 65.152, 65.152, 104.798 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.990 - 1.800 |
R-factor | 0.1939 |
Rwork | 0.191 |
R-free | 0.23980 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a1s |
RMSD bond length | 0.007 |
RMSD bond angle | 1.060 |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.650 |
Number of reflections | 31207 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 25% PEG3350, 0.1M Tris-HCl, pH8.5, 0.1M NaCl |