393D
CRYSTAL STRUCTURE OF TWO SELF-COMPLEMENTARY CHIMERIC DECAMER D(CCGG)R(C)D(GCCGG) AND D(CCGG)R(CG)D(CCGG)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Detector technology | AREA DETECTOR |
| Collection date | 1995-06-13 |
| Detector | SIEMENS |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 24.520, 44.850, 47.580 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.000 |
| Rwork | 0.181 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 3.800 |
| Data reduction software | XENGEN |
| Data scaling software | XENGEN |
| Refinement software | X-PLOR (3.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.049 |
| Number of reflections | 3219 |
| Completeness [%] | 96.0 |
| Redundancy | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | pH 6.00, VAPOR DIFFUSION, HANGING DROP, temperature 291.00K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | NA-CACODYLATE | ||
| 3 | 1 | 1 | COBALT HEXAMINE | ||
| 4 | 1 | 2 | WATER | ||
| 5 | 1 | 2 | MPD |
