35WM

Human Lysine Acetyltransferase KAT2B - Not Shipped

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE VMXi
Synchrotron site	Diamond
Beamline	VMXi
Temperature [K]	293
Detector technology	PIXEL
Collection date	2025-11-17
Detector	DECTRIS EIGER2 X 4M
Wavelength(s)	0.7748
Spacegroup name	P 1 21 1
Unit cell lengths	37.202, 87.711, 60.726
Unit cell angles	90.00, 96.62, 90.00

Refinement procedure

Resolution	60.394 - 1.870
Rwork	0.166
R-free	0.20310
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.688
Data reduction software	xia2.multiplex
Data scaling software	Aimless
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0430 (refmacat 0.4.126))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	87.710	8.970
High resolution limit [Å]	1.870	1.870
Rmerge	0.280
Number of reflections	32019	1556
<I/σ(I)>	10.3
Completeness [%]	100.0
Redundancy	16.8
CC(1/2)	0.984	0.367

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.2	293	PEG 3350, PEG 8000, TRIS HCl