318D
CRYSTAL STRUCTURES OF D(CCGGGCC(BR)5CGG)-HEXAGONAL FORM
Experimental procedure
Source type | ROTATING ANODE |
Temperature [K] | 295 |
Detector technology | AREA DETECTOR |
Collection date | 1995-04-01 |
Detector | SIEMENS-NICOLET |
Spacegroup name | P 61 |
Unit cell lengths | 55.680, 55.680, 46.240 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.000 |
R-factor | 0.162 |
Rwork | 0.162 |
R-free | 0.18000 |
RMSD bond length | 0.020 |
RMSD bond angle | 1.850 |
Data reduction software | XENGEN (V. 2.0) |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.000 |
Rmerge | 0.038 |
Number of reflections | 3193 |
<I/σ(I)> | 15.7 |
Completeness [%] | 58.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 22 * | pH 7.00, VAPOR DIFFUSION, HANGING DROP, temperature 295.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | NA CACODYLATE | ||
3 | 1 | 1 | MGCL2 | ||
4 | 1 | 1 | SPERMINE_HCL | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | 1 (mM) | single stranded |
2 | 1 | drop | sodium cacodylate | 40 (mM) | |
3 | 1 | drop | 5 (mM) | ||
4 | 1 | drop | spermine tetrachloride | 2 (mM) | |
5 | 1 | reservoir | MPD | 50 (%(v/v)) |