30IX
Crystal structure of CSNK1G2 with a covalent compound GCL47
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-02-06 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.000000 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 93.765, 96.110, 184.046 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.100 - 2.900 |
| R-factor | 0.23394 |
| Rwork | 0.231 |
| R-free | 0.29043 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.429 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.100 | 3.030 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Number of reflections | 37325 | 4490 |
| <I/σ(I)> | 12.4 | 1.9 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 13.6 | 14.1 |
| CC(1/2) | 0.999 | 0.810 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 277 | 12% PEG Smear Medium, 0.1 M HEPES pH 7.0, 0.05 M ammonium acetate, and 0.15 M magnesium sulfate |
