2ZVZ
Structure of the periplasmic domain of MotB from Salmonella (crystal form III)
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 35 |
Detector technology | CCD |
Collection date | 2008-02-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.00 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 45.200, 46.240, 173.700 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 44.680 - 2.400 |
R因子 | 0.245 |
Rwork | 0.245 |
R-free | 0.27500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zov |
結合長の平均二乗偏差(RMSD) [Å] | 0.009 |
結合角の平均二乗偏差(RMSD) [度] | 1.800 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | CNS (1.1) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 45.220 | 2.530 |
分解能 [Å] (高) | 2.400 | 2.400 |
独立反射数 | 14884 | |
<I/σ(I)> | 17 | 5.4 |
完全性 [%] | 99.5 | 99.4 |
冗長性 | 5.7 | 5.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 22% PEG MME 2000, 0.1M Acetate, 0.1M MgSO4, pH 4.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |