2YA3
STRUCTURE OF THE REGULATORY FRAGMENT OF MAMMALIAN AMPK IN COMPLEX WITH COUMARIN ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-10 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.943, 124.060, 125.315 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.510 |
R-factor | 0.22463 |
Rwork | 0.223 |
R-free | 0.26271 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v8q |
RMSD bond length | 0.007 |
RMSD bond angle | 1.230 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.200 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.060 | 0.260 |
Number of reflections | 25251 | |
<I/σ(I)> | 18 | 4 |
Completeness [%] | 99.2 | 99.9 |
Redundancy | 3.6 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |