2XTD
Structure of the TBL1 tetramerisation domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-08-26 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 32 1 2 |
Unit cell lengths | 47.886, 47.886, 153.811 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 51.300 - 3.200 |
R-factor | 0.28001 |
Rwork | 0.278 |
R-free | 0.31530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xtc |
RMSD bond length | 0.029 |
RMSD bond angle | 2.002 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.000 | 3.370 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.060 | 0.430 |
Number of reflections | 3503 | |
<I/σ(I)> | 20.2 | 5.1 |
Completeness [%] | 99.8 | 100 |
Redundancy | 6.7 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | 15% MPD, 0.05 M SODIUM ACETATE PH 4.5 |