2WIH
STRUCTURE OF CDK2-CYCLIN A WITH PHA-848125
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-04-28 |
Detector | ADSC CCD |
Spacegroup name | P 62 2 2 |
格子定数 [Å] | 183.000, 183.000, 213.560 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 29.960 - 2.500 |
R因子 | 0.215 |
Rwork | 0.213 |
R-free | 0.25000 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
結合長の平均二乗偏差(RMSD) [Å] | 0.006 |
結合角の平均二乗偏差(RMSD) [度] | 0.900 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNX |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 30.000 | 2.600 |
分解能 [Å] (高) | 2.500 | 2.500 |
Rmerge_l_obs | 0.090 | 0.570 |
独立反射数 | 72932 | |
<I/σ(I)> | 16.1 | 3.7 |
完全性 [%] | 99.7 | 100 |
冗長性 | 7 | 0 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 20% AMMONIUM SULPHATE, 1M KCL, 40MM HEPES PH 7 |