2WIH
STRUCTURE OF CDK2-CYCLIN A WITH PHA-848125
Experimental procedure
| 実験手法 | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-04-28 |
| Detector | ADSC CCD |
| Spacegroup name | P 62 2 2 |
| 格子定数 [Å] | 183.000, 183.000, 213.560 |
| 格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
| 残基 | 29.960 - 2.500 |
| R因子 | 0.215 |
| Rwork | 0.213 |
| R-free | 0.25000 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| 結合長の平均二乗偏差(RMSD) [Å] | 0.006 |
| 結合角の平均二乗偏差(RMSD) [度] | 0.900 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | CNX |
Quality characteristics
| Overall | Outer shell | |
| 分解能 [Å] (低) | 30.000 | 2.600 |
| 分解能 [Å] (高) | 2.500 | 2.500 |
| Rmerge_l_obs | 0.090 | 0.570 |
| 独立反射数 | 72932 | |
| <I/σ(I)> | 16.1 | 3.7 |
| 完全性 [%] | 99.7 | 100 |
| 冗長性 | 7 | 0 |
結晶化条件
| 結晶ID | 方法 | pH | 温度 | 溶液条件 |
| 1 | 20% AMMONIUM SULPHATE, 1M KCL, 40MM HEPES PH 7 |
