Loading
PDBj
メニューPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

2WEA

ACID PROTEINASE (PENICILLOPEPSIN) (E.C.3.4.23.20) COMPLEX WITH PHOSPHONATE INHIBITOR: METHYL[CYCLO-7[(2R)-((N-VALYL) AMINO)-2-(HYDROXYL-(1S)-1-METHYOXYCARBONYL-2-PHENYLETHOXY) PHOSPHINYLOXY-ETHYL]-1-NAPHTHALENEACETAMIDE], SODIUM SALT

1WEA」から置き換えられました
Experimental procedure
Source typeROTATING ANODE
Source detailsOTHER
Temperature [K]110
Detector technologyAREA DETECTOR
Collection date1997-03-22
DetectorSIEMENS-NICOLET X100
Spacegroup nameC 1 2 1
格子定数 [Å]96.330, 46.270, 64.590
格子定数 [度]90.00, 115.10, 90.00
精密化法
残基40.000 - 1.250
R因子0.149
Rwork0.145
R-free0.19200

*

Structure solution methodDIFFERENCE FOURIER METHOD
結合長の平均二乗偏差(RMSD) [Å]0.014
結合角の平均二乗偏差(RMSD) [度]1.454
Data reduction softwareXENGEN
Data scaling softwareXENGEN
Phasing softwareX-PLOR
Refinement softwareTNT
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)40.0001.290
分解能 [Å] (高)1.2501.250
Rmerge_l_obs0.0590.148
Total number of observations203415

*

独立反射数58629
<I/σ(I)>41.285.18
完全性 [%]82.240.47
冗長性3.472.05
結晶化条件
結晶ID方法pH温度溶液条件
1Vapor diffusion, hanging drop

*

4.418-22

*

used macroseeding, Fraser, M.E., (1992) Biochemistry, 31, 5201.

*

文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11dropammonium sulfate34-40 (%sat)
21drop0.1 (M)
31dropcomplex10 (mg/ml)

225158

件を2024-09-18に公開中

PDB statisticsPDBj update infoContact PDBjnumon