Loading
PDBj
メニューPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

2GUB

Crystal Structure of Metal Free D-Xylose Isomerase.

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]279
Detector technologyAREA DETECTOR
Collection date1995-11-15
DetectorSIEMENS-NICOLET X100
Wavelength(s)1.5418
Spacegroup nameI 2 2 2
格子定数 [Å]93.800, 99.500, 102.800
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基70.710 - 1.800
R因子0.16124
Rwork0.160
R-free0.19327
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)1XIB without metal ions and solvent
結合長の平均二乗偏差(RMSD) [Å]0.020
結合角の平均二乗偏差(RMSD) [度]1.739
Data reduction softwareDATCOL
Data scaling softwareXDS
Refinement softwareREFMAC (5.2.0005)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)70.7101.900
分解能 [Å] (高)1.8001.800
独立反射数40569
完全性 [%]0.886.6
結晶化条件
結晶ID方法pH温度溶液条件
1SMALL TUBES8279Crystallization from solution containing metal free enzyme at 20 mg/ml, 0.8M AmSO4, 2mM Pipes. Crystallization occurred over 2 day period in sealed tubes., pH 8.0, SMALL TUBES, temperature 279K

225158

件を2024-09-18に公開中

PDB statisticsPDBj update infoContact PDBjnumon