2GCP
Crystal structure of the human RhoC-GSP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 59.435, 59.435, 138.090 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.550 - 2.150 |
R-factor | 0.16229 |
Rwork | 0.159 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1z2c |
RMSD bond length | 0.016 |
RMSD bond angle | 1.733 |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.593 | 2.270 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.122 | 0.583 |
Total number of observations | 24100 | |
Number of reflections | 14205 | 2019 |
<I/σ(I)> | 6.1 | 1.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 11.8 | 11.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.8 | 291.15 | 3M Sodium Chloride, 0.1M Sodium Acetate, pH 4.8, VAPOR DIFFUSION, HANGING DROP, temperature 291.15K |