2FNE
The crystal structure of the 13th PDZ domain of MPDZ
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-12-09 |
Detector | MARRESEARCH |
Wavelength(s) | 0.97900 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.943, 62.380, 53.128 |
Unit cell angles | 90.00, 106.26, 90.00 |
Refinement procedure
Resolution | 39.500 - 1.830 |
R-factor | 0.19415 |
Rwork | 0.190 |
R-free | 0.24293 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2byg |
RMSD bond length | 0.015 |
RMSD bond angle | 1.556 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.500 | 1.950 |
High resolution limit [Å] | 1.830 | 1.830 |
Rmerge | 0.051 | 0.475 |
Number of reflections | 26605 | |
<I/σ(I)> | 2.15 | |
Completeness [%] | 99.9 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 298 | 8% PEG P3350, 0.1M acetate, pH 4.6, VAPOR DIFFUSION, SITTING DROP, temperature 298K |