2C4G
STRUCTURE OF CDK2-CYCLIN A WITH PHA-533514
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-11-20 |
Detector | ADSC CCD |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 191.985, 191.985, 205.880 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.930 - 2.700 |
Rwork | 0.233 |
R-free | 0.25000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1fin |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNX (2002) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.080 | 0.700 |
Number of reflections | 61565 | |
<I/σ(I)> | 17 | 2.4 |
Completeness [%] | 99.7 | 99.4 |
Redundancy | 5.2 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 20% AMMONIUM SULPHATE, 1M KCL, 40MM HEPES PH 7 |