2BKZ
STRUCTURE OF CDK2-CYCLIN A WITH PHA-404611
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-02-22 |
Detector | ADSC CCD |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 183.862, 183.862, 214.572 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.800 - 2.600 |
Rwork | 0.230 |
R-free | 0.25900 |
Structure solution method | OTHER |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNX (2002) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.080 | 0.530 |
Number of reflections | 66033 | |
<I/σ(I)> | 18.2 | 3 |
Completeness [%] | 99.7 | 99.8 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 20% AMMONIUM SULPHATE, 1M KCL, 40MM HEPES PH 7 |