2ZNY
Crystal structure of the FFRP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 95 |
| Detector technology | CCD |
| Collection date | 2007-10-17 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 102.310, 73.500, 103.060 |
| Unit cell angles | 90.00, 98.47, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.590 |
| R-factor | 0.254 |
| Rwork | 0.254 |
| R-free | 0.25800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ri7 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.680 |
| High resolution limit [Å] | 2.590 | 2.590 |
| Rmerge | 0.080 | 0.223 |
| Number of reflections | 47467 | |
| <I/σ(I)> | 19.1 | 4.8 |
| Completeness [%] | 95.2 | 98.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 294 | 25% PEG 3350, 0.3M CaCl2, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 294K |
