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2ZGO

Crystal structure of AAL mutant H59Q complex with lactose

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU FR-E+ SUPERBRIGHT
Temperature [K]98
Detector technologyIMAGE PLATE
Collection date2006-12-28
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.5418
Spacegroup nameP 1
Unit cell lengths40.660, 42.850, 55.970
Unit cell angles101.88, 98.72, 117.24
Refinement procedure
Resolution29.710 - 2.000
R-factor0.2
Rwork0.200
R-free0.23900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2zgl
RMSD bond length0.006
RMSD bond angle1.400
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareCNS (1.2)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]29.7102.110
High resolution limit [Å]2.0002.000
Rmerge0.0270.045
Number of reflections20227
<I/σ(I)>31.623.5
Completeness [%]95.091.1
Redundancy3.23.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.529825% PEG3350, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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